Preparation of silica gel from rice husk ash using microwave heating
คำสำคัญ:
Rice husk ash, Silica gel, Waste utilization, Microwave, Dielectric heating, Sodium silicateบทคัดย่อ
The purpose of this research is to separate silica gel from rice husk ash by microwave heating. The experiments were performed by heating rice husk ash in sodium hydroxide solution with various concentrations in microwave oven for 5 or 10 minutes. The obtained sodium silicate was neutralized to give silica gel. The best condition for silica gel production was the reaction with 2.0 M sodium hydroxide at microwave power of 800 W for 10 minutes. The ability of silica gel as desiccant was investigated by adsorption test. The results showed that silica gel prepared by low concentration of sodium hydroxide solution had the highest ability of water adsorption. The power of microwave and volume of reactions seemed to have only little effect.Downloads
เอกสารอ้างอิง
Della, V.P., Kühn, I. and Hotza, D. 2002. Rice husk ash as an alternate source for active silica production. Mater. Lett. 57: 818-821.
Real C., Alcalá M.D. and Criado, J.M. 1996. Preparation of Silica from rice husks. J. Am. Ceram. Soc. 79(8) : 2012-2016.
Kalapathy, U., Proctor, A. and Shultz, J. 2000. A simple method for production of pure silica from rice hull ash. Bioresour. Technol. 73(3) : 257-262.
Kalapathy, U., Proctor , A. and Shultz , J. 2002. An improved method for production of silica from rice hull ash. Bioresour. Technol. 85(3) : 285-289.
Foletto, E.L., Gratieri, E., de Oliveira, L.H. and Jahn, S.L., 2006. Conversion of rice hull ash into soluble sodium silicate. Mater. Res. 9(3):335-338.
Rungrodnimitchai, S. and Supjaroenkul, U, 2009. Modification of rice straw for heavy metal ion adsorbents by MW heating. Prague Meetings on Macromolecules. Prague, Republic of Chez.
Novotny, R., Hoff, A. and Schuertz, J. 1991. Process for hydrothermal production of sodium silicate solutions. US. Patent. no 545000933
ดาวน์โหลด
เผยแพร่แล้ว
วิธีการอ้างอิง
ฉบับ
บท
การอนุญาต
ลิขสิทธิ์ (c) 2017 Journal of Metals, Materials and Minerals
This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.
Authors who publish in this journal agree to the following terms:
- Authors retain copyright and grant the journal right of first publication with the work simultaneously licensed under a Creative Commons Attribution License that allows others to share the work with an acknowledgment of the work's authorship and initial publication in this journal.
- Authors are able to enter into separate, additional contractual arrangements for the non-exclusive distribution of the journal's published version of the work (e.g., post it to an institutional repository or publish it in a book), with an acknowledgment of its initial publication in this journal.