The finished polyester fabric with hot NH4OH pretreatment and mixed ZnO-Zn(OH)2 nanoparticles for hydrophobic property

Samroeng NARAKAEW; Sittipong AU-PREE; Wipanoot BAISON; Siwat THUNGPRASERT; Itsariya WATTALO; Pranpreeya JAIPOR; Theeraporn PROMANAN; Sukee SUKDEE; Pakorn SANTAKIJ; Chainet CHANOGKUN; Kanjana RUTTANATEERAWICHIEN; Aphiruk CHAISENA; Pattama APICHAI; Phiphop NARAKAEW

doi:10.55713/jmmm.v32i1.1226

Authors

Samroeng NARAKAEW Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Sittipong AU-PREE Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Wipanoot BAISON Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Siwat THUNGPRASERT Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Itsariya WATTALO Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Pranpreeya JAIPOR Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Theeraporn PROMANAN Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Sukee SUKDEE Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Pakorn SANTAKIJ Department of Information Technology, Lampang Rajabhat University, Lampang, 52100, Thailand
Chainet CHANOGKUN Department of Communicative Thai for Foreigners, Lampang Rajabhat University, Lampang, 52100, Thailand
Kanjana RUTTANATEERAWICHIEN Department of Digital Business Management, Lampang Rajabhat University, Lampang, 52100, Thailand
Aphiruk CHAISENA Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Pattama APICHAI Department of Physics, Lampang Rajabhat University, Lampang, 52100, Thailand
Phiphop NARAKAEW Department of Physics, Lampang Rajabhat University, Lampang, 52100, Thailand

DOI:

https://doi.org/10.55713/jmmm.v32i1.1226

Keywords:

The finished polyester fabric, Hot NH4OH pretreatment, Mixed Zn(OH)2/ZnO nanoparticles, Hydrophobic property

Abstract

This work aims to modify the hydrophobic coated polyester fabrics using 2%w/v ammonium hydroxide (NH₄OH) at 90℃ prior and subsequently dipped in two difference aqueous zinc solution batchs containing 0.6%w/v zinc precursors with/without starch and NH₄OH, finally dehydration, and characterized by the attenuated total reflection - Fourier transform Infrared (ATR-FTIR) and Raman spectroscopy (Raman), X-ray diffraction (XRD), Field emission scanning electron microscope (FE-SEM), Energy dipersive spectrometry (EDX), and Water contact angle (WCA) of 10 mL dropping at 23℃ and humidity of 63%. Raman spectra and XRD patterns results showed e-zinc hydroxide (e-Zn(OH)₂), zinc oxide nanoparticle (ZnO NP) and ZnO-starch nanocomposite crystallized in the orthorhombic and hexagonol wurzite structure, respectively. The increasing intensities of Raman vibrational modes at 369 cm^-1 and 750 cm^-1 confirmed the increased of e-Zn(OH)₂ content with additional starch, therefore, WCA trend of those finished fabric surfaces decreased. WCA optimum of 138° before washing and 136° after 5 washing cycles of the treated fabric which was activated by NH₄OH acts as scourer and also as promoter of e-Zn(OH)₂/ZnO NPs as revealed from ATR-FTIR result. While, other observed lower hydrophobic property after 5 washing cycles due to the hydroplilic ZnO-starch nanocomposite.e-Zn(OH)₂/ZnO NPs. While others, there were observed lower hydrophobic property after 5 washing cycles due to the hydroplilic ZnO-starch nanocomposite.

Downloads

Download data is not yet available.

References

M. Shaban, F. Mohamed, and S. Abdallah., “Production and characterization of superhydrophobic and antibacterial coated fabrics utilizing ZnO nanocatalyst,” Scientific Reports, vol. 8, pp. 1-15, 2018.

N. P. Prorokova, T. Yu. Kumeeva, D. P. Kiryukhin, L. N. Nikitin, and V. M. Buznik, “Imparting enhanced hydrophobicity to polyester fabrics: Formation of ultrathin water-repelling coatings on the fiber surface,” Rossiiskii Khimicheskii Zhurnal, vol. 55, pp.14-23, 2012.

S .S. Latthe, A .B. Gurav, C. S. Maruti, and R. S. Vhatkar, “Recent progress in preparation of superhydrophobic surfaces: A review,” Journal of Surface Engineered Materials and Advanced Technology, vol. 22, pp. 76-94, 2012.

J. T. Han, X. R. Xu, and K. W. Cho, “Diverse access to artificial superhydrophobic surfaces using block copolymers,” Langmuir, vol. 21, pp. 6662-6665, 2005.

J. Shirtcliffe, G. McHale, M. I. Newton, G. Chabrol, and C. C. Perry, “Dual-scale roughness produces unusually water-repellent surfaces,” Advanced Materials, vol. 16, pp. 1929-1932, 2004.

H. S. Hwang, S. B. Lee, and I. Park, “Fabrication of raspberry-like superhydrophobic hollow silica particles,” Materials Letters, vol. 64, pp. 2159-2162, 2010.

Y. H. Huang, J. T. Wu, and S. Y. Yang, “Direct fabricating patterns using stamping transfer process with PDMS mold of hydrophobic nanostructures on surface of micro-cavity,” Microelectronic Engineering, vol. 88, pp. 849-854, 2011.

T. Yang, H. Tian, and Y. Chen, “Preparation of superhydrophobic silica films with honeycomb-like structure by emulsion method,” Journal of Sol-Gel Science and Technology, vol. 49, pp. 243-246, 2009.

H. Kinoshita, A. Ogasahara, Y. Fukuda, and N. Ohmae, “Superhydrophobic/superhydrophilic micropatterning on a carbon nanotube film using a Laser Plasma-type hyperthermal atom beam facility,” Carbon, vol. 48, pp. 4403-4408, 2010.

Z. G. Guo, J. Fang, J. C. Hao, Y. M. Liang, and W. M. Liu, “A novel approach to stable superhydrophobic surfaces,” ChemPhysChem, vol. 7, pp. 1674-1677, 2006.

K. K. Lau, J. Bico, K. B. K. Teo, M. Chowalla, G. A. J. Amaratung, W. I. Milne, G. H. McKinley, and K. K. Gleason, “Superhydrophobic carbon nanotube forests,” Nano Letters, vol. 3, pp. 1701-1705, 2003.

F. Mumm, A. T. J. van Helvoort, and P. Sikoski, “An easy route to superhydrophobic copper-based droplet microfluidic systems,” ACS Nano, vol. 3, pp. 2647-2652, 2009.

S. S. Latthe, H. Imai, V. Ganesan, and A.V. Rao, “Super-hydrophobic silica films by sol-gel co-precursor method”, Applied Surface Science, vol. 256, pp. 217-222, 2009.

S. S. Latthe, H. Hirashima, and A. V. Rao, “TEOS based water repellent silica films obtained by a co-precursor sol-gel method,” Smart Materials Structures, vol. 18, p. 095017, 2009.

A. V. Rao, S. S. Latthe, C. Kappenstein, V. Ganesan, M. C. Rath, and S. N. Sawant, “Wetting behavior of high energy electron irradiated porous superhydrophobic silica films,” Applied Surface Science, vol. 257, pp. 3027-3032, 2011.

V. V. Ganbavle, U. K. H. Bangi, S. S. Latthe, S. A. Mahadik, and A. V. Rao, “Self-cleaning silica coatings on glass by single step sol-gel route,” Surface and Coatings Technology, vol. 205, pp. 5338-5344, 2011.

R. Furstner, W. Barthlott, C. Neinhuis, and P. Walzel, “Wetting and self-cleaning properties of artificial super-hydrophobic surface,” Langmuir, vol. 21, pp. 956-961, 2005.

M. Ma, Y. Mao, M. Gupta, K. K. Gleason, and G.C. Rutledge, “Superhydrophobic fabrics produced by electrospinning and chemical vapor deposition,” Macromolecules, vol. 38, pp. 9742-9748, 2005.

X. Zhang, Y. Guo, P. Zhang, Z. Wu, and Z. Zhang, “Super-hydrophobic CuO@Cu2S nanoplate vertical arrays on copper surfaces,” Materials Letters, vol. 64, pp. 1200-1203, 2010.

S. Nourbakhsh, M. Montazer, and Z. Khandaghabadi, “Zinc oxide nano particles coating on polyester fabric functionalized through alkali treatment,” Journal of Industrial Textiles, vol. 47, pp. 1-18, 2016.

P. Kampeerapappun, “Effect of zinc oxide loaded polyester fibers on the color, mechanical properties and antibacterial action of woven fabric,” Journal of Metals, Materials and Minerals, vol. 28, pp. 33-40, 2018.

M. Wang, M. Zhang, L. Pang, C. Yang, Y. Zhang, J. Hu, and G. Wu, “Fabrication of highly durable polysiloxane-Zinc oxide (ZnO) coated polyethylene terephthalate (PET) fabric with improved ultraviolet resistance, hydrophobicity, and thermal resistance,” Journal of Colloid and Interface Science, vol. 534, pp. 91-100, 2019.

G. Achagri, Y. Essamlali, O. Amadine, M. Majdoub, A. Chakir, and M. Zahouily, “Surface modification of highly hydrophobic polyester fabric coated with octadecylamine functionalized graphene nanosheets,” RSC Advances, vol. 10, pp. 24941-24950, 2020.

D. E. A. Boryo, K. A. Bello, A. Q. Ibrahim, A. I. Ezeribe, F. I. Omizegba, and P. U. Offodile, “Effect of alternative scouring agents on mechanical properties of cotton/polyester blend fabric,” The International Journal of Engineering and Science, vol. 2, pp. 121-134, 2013.

H. Poortavasoly, and M. Montazer, “Functional polyester fabric through simultaneous aminolysis and nano ZnO synthesis,” Journal of Ultrafined and Nanostructured Materials, vol. 47, no. 2, pp. 113-119, 2014.

M. T. Thein, S.-Y. Pung, A. Aziz, and M. Itoh, “The role of ammonia hydroxide in the formation of ZnO hexagonal nanodisks using sol-gel technique and their photocatalytic study,” Journal of Experimental Nanoscience, vol. 10, pp. 1-15, 2014.

J. Ma, W. Zhu, Y. Tian, and Z. Wang, “Preparation of zinc oxide-starch nanocomposite and its application on coating,” Nanoscale Research Letters, vol. 11, pp. 1-9, 2016.

D. Puchowicz, and M. Cieslak, "Raman Spectroscopy in the Analysis of Textile Structures", in Recent Developments in Atomic Force Microscopy and Raman Spectroscopy for Materials Characterization. London, United Kingdom: IntechOpen, 2021 [Online]. Available: https://www.intechopen.com/chapters/78288.

A. M. Al-Sabagh, F. Z. Yehia, Gh. Eshaq, A. M. Rabie, A. E. ElMetwally, “Greener routes for recycling of polyethylene terephthalate,” Egyptian Journal of Petroleum, vol. 25, pp. 53-64, 2016.

A. Carton, S. Abdelouhab, G. Renaudin, P. Rabu and M. François, “Structure of zinc hydroxy-terephthalate: Zn3(OH)4(C8H4O4),” Solid State Sciences, vol. 8, pp. 958-963, 2006.

M. Šĭrek and J. Jiroušek, “The method of chemical recycling of polyethylene terephthalate waste,” Patent international number: WO 01/68581 A2, 2001.

V. Russo, M. Ghidelli, P. Gondoni, C. S. Casari, and A. L. Bassi, “Multi-wavelength Raman scattering of nanostructured Al-doped zinc oxide,” Journal of Applied Physics, vol. 115, p. 073508, 2014.

A.-K. Elger, and C. Hess, “Application of Raman spectroscopy to working gas sensors: From in situ to operando studies,” Sensors, vol. 19, pp. 5075, 2019.

E. A. Gavrilenko, D. A. Goncharova, I. N. Lapin, A. L. Nemoykina, V. A. Svetlichnyi, A. A. Aljulaih, N. Mintcheva, and S. A. Kulinich, “Comparative study of physicochemical and antibacterial properties of ZnO nanoparticles prepared by laser ablation of Zn target in water and air,” Materials, vol. 12, pp. 1-30, 2019.

M. Wang, L. Jiang, E. J. Kim, and S. H. Hahn, “Electronic structure and optical properties of Zn(OH)2: LDA+U calculations and intense yellow luminescence,” RSC Advances, vol. 5, pp. 87496-87503, 2015.

E. Hager, C. Farber, and D. Kurouski, “Forensic identification of urine on cotton and polyester fabric with a hand-held Raman spectrometer,” Forensic Chemistry, vol. 9, pp. 44-49, 2018.

M. Sha, D. Zhang, Z. Zhang, J. Wei, Y. Chen, M. Wang, and J. Lui, “Improving Raman spectroscopic identification of rice varieties by feature extraction,” Journal of Raman Spectroscopy, vol. 51, pp. 1-9, 2020.

R. B. Corey, and R. W. G. Wyckoff, “The crystal structure of zinc hydroxide,” Zeitschrift für Kristallographie – Crystalline Materials, vol. 86, pp. 8-18, 1933.

S. V. Nistor, D. Ghica, M. Stefan, I. Vlaicu, J. N. Barascu, and C. Bartha, “Magnetic defects in crystalline Zn(OH)2 and nanocrystalline ZnO resulting from its thermal decomposition,” Journal of Alloys and Compounds, vol. 548, pp. 222-227, 2013.

M. M. AbdElhady, “Preparation and characterization of chitosan/zinc oxide nanoparticles for imparting antimicrobial and UV protection to cotton fabric,” International Journal of Carbohydrate Chemistry, Article ID 840591, 2012.

D. Shao, and Q. Wei, “Microwave-assisted rapid preparation of nano-ZnO/Ag composite functionalized polyester nonwoven membrane for improving its UV shielding and antibacterial properties,” Materials, vol. 11, pp. 1412, 2018.

A. Top, and H. Çetinkaya, “Zinc oxide and zinc hydroxide formation via aqueous precipitation: Effect of the preparation route and lysozyme addition,” Materials Chemistry and Physics, vol. 167, pp. 77-87, 2015.

M. S. Han, Y. Park, and C.H. Park, “Development of super-hydrophobic polyester Fabrics using alkaline hydrolysis and coating with fluorinated polymers,” Fibers and Polymers, vol. 17, pp. 241-247, 2016.