The finished polyester fabric with hot NH4OH pretreatment and mixed ZnO-Zn(OH)2 nanoparticles for hydrophobic property

Samroeng NARAKAEW; Sittipong AU-PREE; Wipanoot BAISON; Siwat THUNGPRASERT; Itsariya WATTALO; Pranpreeya JAIPOR; Theeraporn PROMANAN; Sukee SUKDEE; Pakorn SANTAKIJ; Chainet CHANOGKUN; Kanjana RUTTANATEERAWICHIEN; Aphiruk CHAISENA; Pattama APICHAI; Phiphop NARAKAEW

doi:10.55713/jmmm.v32i1.1226

ผู้แต่ง

Samroeng NARAKAEW Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Sittipong AU-PREE Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Wipanoot BAISON Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Siwat THUNGPRASERT Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Itsariya WATTALO Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Pranpreeya JAIPOR Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Theeraporn PROMANAN Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Sukee SUKDEE Department of Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Pakorn SANTAKIJ Department of Information Technology, Lampang Rajabhat University, Lampang, 52100, Thailand
Chainet CHANOGKUN Department of Communicative Thai for Foreigners, Lampang Rajabhat University, Lampang, 52100, Thailand
Kanjana RUTTANATEERAWICHIEN Department of Digital Business Management, Lampang Rajabhat University, Lampang, 52100, Thailand
Aphiruk CHAISENA Department of Applied Chemistry and Center for Innovation in Chemistry, Lampang Rajabhat University, Lampang, 52100, Thailand
Pattama APICHAI Department of Physics, Lampang Rajabhat University, Lampang, 52100, Thailand
Phiphop NARAKAEW Department of Physics, Lampang Rajabhat University, Lampang, 52100, Thailand

DOI:

https://doi.org/10.55713/jmmm.v32i1.1226

คำสำคัญ:

The finished polyester fabric, Hot NH4OH pretreatment, Mixed Zn(OH)2/ZnO nanoparticles, Hydrophobic property

บทคัดย่อ

This work aims to modify the hydrophobic coated polyester fabrics using 2%w/v ammonium hydroxide (NH₄OH) at 90℃ prior and subsequently dipped in two difference aqueous zinc solution batchs containing 0.6%w/v zinc precursors with/without starch and NH₄OH, finally dehydration, and characterized by the attenuated total reflection - Fourier transform Infrared (ATR-FTIR) and Raman spectroscopy (Raman), X-ray diffraction (XRD), Field emission scanning electron microscope (FE-SEM), Energy dipersive spectrometry (EDX), and Water contact angle (WCA) of 10 mL dropping at 23℃ and humidity of 63%. Raman spectra and XRD patterns results showed e-zinc hydroxide (e-Zn(OH)₂), zinc oxide nanoparticle (ZnO NP) and ZnO-starch nanocomposite crystallized in the orthorhombic and hexagonol wurzite structure, respectively. The increasing intensities of Raman vibrational modes at 369 cm^-1 and 750 cm^-1 confirmed the increased of e-Zn(OH)₂ content with additional starch, therefore, WCA trend of those finished fabric surfaces decreased. WCA optimum of 138° before washing and 136° after 5 washing cycles of the treated fabric which was activated by NH₄OH acts as scourer and also as promoter of e-Zn(OH)₂/ZnO NPs as revealed from ATR-FTIR result. While, other observed lower hydrophobic property after 5 washing cycles due to the hydroplilic ZnO-starch nanocomposite.e-Zn(OH)₂/ZnO NPs. While others, there were observed lower hydrophobic property after 5 washing cycles due to the hydroplilic ZnO-starch nanocomposite.

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