Study of titanium alloy Ti–Al–Zr–Nb–V during heating under deformation and its phase transformation features

Aidar KENZHEGULOV; Axaule MAMAEVA; Aleksander PANICHKIN; Akerke IMBAROVA; Balzhan KSHIBEKOVA; Rashida AUBAKIROVA; Natasha  SATKANOVA; Nazgul  TOIYNBAEVA

doi:10.55713/jmmm.v34i2.1908

Authors

Aidar KENZHEGULOV JSC "Institute of Metallurgy and Ore Beneficiation", Almaty, Republic of Kazakhstan
Axaule MAMAEVA JSC "Institute of Metallurgy and Ore Beneficiation", Almaty, Republic of Kazakhstan https://orcid.org/0000-0002-9659-8152
Aleksander PANICHKIN JSC "Institute of Metallurgy and Ore Beneficiation", Almaty, Republic of Kazakhstan https://orcid.org/0000-0002-2403-8949
Akerke IMBAROVA JSC "Institute of Metallurgy and Ore Beneficiation", Almaty, Republic of Kazakhstan https://orcid.org/0000-0002-9366-314X
Balzhan KSHIBEKOVA JSC "Institute of Metallurgy and Ore Beneficiation", Almaty, Republic of Kazakhstan https://orcid.org/0000-0002-5944-7865
Rashida AUBAKIROVA JSC "Institute of Metallurgy and Ore Beneficiation", Almaty, Republic of Kazakhstan
Natasha SATKANOVA Satbayev University, Almaty, Republic of Kazakhstan
Nazgul TOIYNBAEVA Satbayev University, Almaty, Republic of Kazakhstan

DOI:

https://doi.org/10.55713/jmmm.v34i2.1908

Keywords:

superplasticity, microstructure, alloy, optical microscopy, scanning electron microscopy

Abstract

An alloy based on Ti–Al–Zr–Nb–V was prepared and its deformation behavior at elevated temperatures was studied. The microstructure and phase of the alloys were characterized by optical microscopy, scanning electron microscopy, thermal analysis, and mechanical testing. The results showed that the Ti–Al–Zr–Nb–V alloy, when stretched, exhibits a superplasticity effect in the range of 975℃ to 1100℃, with an elongation of up to 400%. It was found that superplasticity develops in the temperature region of the α+β→β transition and is accompanied by a change in grain size and redistribution of alloying elements among phases.

Downloads

Download data is not yet available.

References

. L. Sheng, Y. Yang, C. Lai, X. Chen, and T. Xi, "Microstructure evolution of a Ti–Al–Sn–Zr based alloy during the hot compression deformation," Materials express, vol. 9, pp. 1127-1133, 2019. DOI: https://doi.org/10.1166/mex.2019.1599

. M. Jayaprakash, D. H. Ping, and Y. Yamabe-Mitarai, "Effect of Zr and Si addition on high temperature mechanical properties of near-Ti–Al–Zr–Sn based alloys," Materials Science & Engineering A, vol. 612, pp. 456-461, 2014. DOI: https://doi.org/10.1016/j.msea.2014.06.078

. A. Mamaeva, A. Kenzhegulov, P. Kowalewski, and W. Wieleba, "Investigation of hydroxyapatite-titanium composite properties during heat treatment," Acta of Bioengineering and Biomechanics, vol. 19, no. 4, pp. 161-169, 2017.

. M. A. Alipovna, K. A. Karaulovich, P. A. Vladimirovich, A. Z. Zhanuzakovich, B. Kshibekova, W. Wieleba, T. Lesniewski, and N. Bakhytuly, "The study of the tribological properties under high contact pressure conditions of TiN, TiC and TiCN coatings deposited by the magnetron sputtering method on the AISI 304 stainless steel substrate," Materials Science- Poland, vol. 41, no. 1, pp. 1-14, 2023. DOI: https://doi.org/10.2478/msp-2022-0055

. S. L. Semiatin, V. Seetharaman, and I. Weiss, "Hot workability of titanium and titanium aluminide alloys-an overview," Materials Science & Engineering A, vol. 243, no. 1-2, pp. 1-24, 1998. DOI: https://doi.org/10.1016/S0921-5093(97)00776-4

. E. Alabort, D. Putman, and R. C. Reed, "Superplasticity in Ti–6Al–4V: Characterisation modelling and applications," Acta Materialia, vol. 95, pp. 428-442, 2015. DOI: https://doi.org/10.1016/j.actamat.2015.04.056

. A. V. Sergueeva, V. V. Stolyarov, R. Z. Valiev, and A. K. Mukherjee, "Advanced mechanical properties of pure titanium with ultrafine grained structure," Scripta Materialia, vol. 45, pp. 747-752, 2001. DOI: https://doi.org/10.1016/S1359-6462(01)01089-2

. V. F. Korshak, and Yu. А. Shapovalov, "Some aspects of superplastic flow of eutectic alloys related to metastability," Physics of metals and metallurgist, vol. 107, no. 4, pp. 422-428, 2009. (Rus) DOI: https://doi.org/10.1134/S0031918X09040103

. V. P. Poida, V. V. Bryukhovetskii, A. V. Poida, R. I. Kuznetsova, V. F. Klepikov, and D. L. Voronov, "Morphology and mechanisms of the formation of fiber structures upon high-temperature superplastic deformation of aluminum alloys," The Physics of Metals and Metallography A, vol. 103, no. 4, pp. 414-423, 2007. DOI: https://doi.org/10.1134/S0031918X07040151

. A. E. Geckinli, "Grain boundary sliding model for superplastic deformation," Metal science, vol. 17, no. 1, pp. 12-18, 1983. DOI: https://doi.org/10.1179/030634583790427504

. T. G. Langdon, "Seventy-five years of superplasticity: historic developments and new opportunities," Journal of materials science, vol. 44, no. 22, pp. 5998-6010, 2009. DOI: https://doi.org/10.1007/s10853-009-3780-5

. S. Roy, and S. Suwas, "The influence of temperature and strain rate on the deformation response and microstructural evolution during hot compression of a titanium alloy Ti–6Al–4V–0.1 B," Journal of Alloys and Compounds, vol. 548, pp. 110-125, 2013. DOI: https://doi.org/10.1016/j.jallcom.2012.08.123

. E. Alabort, D. Barba, M. R. Shagiev, M. A. Murzinova, R. M. Galeyev, O. R. Valiakhmetov, A. F. Aletdinov, and R. C. Reed, "Alloys-by-design: application to titanium alloys for optimal superplasticity," Acta Materialia, vol. 178, pp. 275-287, 2019. DOI: https://doi.org/10.1016/j.actamat.2019.07.026

. Q. Bai, J. G. Lin, T. A. Dean, D. S. Balint, T. Gao, and Z. Zhang, "Modelling of dominant softening mechanisms for Ti-6Al-4V in steady state hot forming conditions," Materials Science and Engineering A, vol. 559, pp. 352-358, 2013. DOI: https://doi.org/10.1016/j.msea.2012.08.110

. Q. J. Sun, G. C. Wang, and M. Q. Li, "The superplasticity and microstructure evolution of TC11 titanium alloy," Materials & Design, vol. 32, no. 7, pp. 3893-3899, 2011. DOI: https://doi.org/10.1016/j.matdes.2011.02.062

. S. Li, J. H. Lim, I. U. Rehman, W. T. Lee, J. G. Kim, J. S. Oh, T. Lee, and T. H. Nam, "Tuning the texture characteristics and superelastic behaviors of Ti–Zr–Nb–Sn shape memory alloys by varying Nb content," Materials Science and Engineering A, vol. 845, pp. 143243, 2022. DOI: https://doi.org/10.1016/j.msea.2022.143243

. J. Fu, H. Y. Kim, and S. Miyazaki, "Effect of annealing temperature on microstructure and superelastic properties of a Ti-18Zr-4.5 Nb-3Sn-2Mo alloy," Journal of the mechanical behavior of biomedical materials, vol. 65, pp. 716-723, 2017. DOI: https://doi.org/10.1016/j.jmbbm.2016.09.036

. L. Kong, B. Wang, X. Meng, and Z. Gao, "Superelasticity by introductions of Cr into the Ti-Zr-Nb-Sn strain glass alloy toward the elastocaloric application, " Journal of Alloys and Compounds, vol. 935, pp. 168156, 2023. DOI: https://doi.org/10.1016/j.jallcom.2022.168156

. R. Kapoor, J. K. Chakravartty, C. C. Gupta, and S. L. Wadekar, "Characterization of superplastic behaviour in the (α+β) phase field of Zr–2.5 wt.% Nb alloy," Materials Science and Engineering A, vol. 392, no. 1-2, pp. 191-202, 2005. DOI: https://doi.org/10.1016/j.msea.2004.09.023

. W. D. Zhang, Z. Wu, Y. Liu, H. Bei, B. Liu, and J. Qiu, "Plastic deformation mechanism of Ti–Nb–Ta–Zr–O alloy at cryogenic temperatures," Materials Science and Engineering A, vol. 765, pp. 138293, 2019. DOI: https://doi.org/10.1016/j.msea.2019.138293

. W. Wang, X. Zhang, and J. Sun, "Phase stability and tensile behavior of metastable Ti–V–Fe and Ti–V–Fe–Al alloys," Materials Characterization, vol. 142, pp. 398-405, 2018. DOI: https://doi.org/10.1016/j.matchar.2018.06.008